Teaching GuideTerm Faculty of Science |
Grao en Nanociencia e Nanotecnoloxía |
Subjects |
Synthesis and Preparation of Nanomaterials |
Contents |
Identifying Data | 2023/24 | |||||||||||||
Subject | Synthesis and Preparation of Nanomaterials | Code | 610G04020 | |||||||||||
Study programme |
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Descriptors | Cycle | Period | Year | Type | Credits | |||||||||
Graduate | 2nd four-month period |
Second | Obligatory | 6 | ||||||||||
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Topic | Sub-topic |
Classification of materials. | Classification of materials. |
Synthesis techniques and preparation of nanomaterials | Fundamentals of nanomaterials synthesis by top-down and bottom-up techniques. General aspects: nucleation and growth; stability. Use of controlled environment laboratories (clean room). Main methods of synthesis of nanoparticles, carbon nanostructures, nanostructured surfaces, mesoporous materials, others. |
Basic characterization of nanomaterials | X-ray diffraction of crystalline powder. Thermal methods (thermogravimetric and thermodifferential analysis). Electron microscopy (transmission and scanning). |
Measurement of particle size and Z-potential | Fundamentals of Dynamic Light Scattering (DLS) technique. Fundamentals of Zeta Potential measurement. |
PREPARATION AND CHARACTERIZATION OF VARIOUS NANOMATERIALS | Selection of the synthesis method, based on the characteristics of the material to be prepared. Selection of the conditions and materials necessary for the synthesis (reagents, previous calculations, material, assemblies...). Evaluation of the risks associated with the experiment and their prevention. Experimental procedure of synthesis. Selection and/or handling of basic instrumental techniques for its characterization. Interpretation of the results of the characterization. Elaboration of the laboratory notebook. Elaboration and presentation of the final report. |
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