Identifying Data

2016/17

Subject (*)

Profundización en Química Analítica

Code

610509001

Study programme

Mestrado en Investigación Química e Química Industrial (plan 2016)

Descriptors

Cycle

Period

Year

Type

Credits

Official Master's Degree

Yearly

First

Obligatoria

Language

Spanish

Teaching method

Face-to-face

Prerequisites

Department

Química Analítica

Coordinador

Muniategui Lorenzo, Soledad

E-mail

soledad.muniategui@udc.es

Lecturers

Carlosena Zubieta, Alatzne

Muniategui Lorenzo, Soledad

E-mail

alatzne.carlosena@udc.es

soledad.muniategui@udc.es

Web

General description

O obxectivo deste materia é a adquisión duhna formación completa e integrada dos métodos analíticos empregados ao longo de todo o proceso analítico incluíndo o estudo de metodoloxías para o muestreo, a preparación de mostras, determinación de analitos e tratamento e interpretación de resultados.
Para isto se amosará aos alumnos unha visión xeral dos métodos analíticos e da súa selección e aplicación para a resolución de problemas reales.
Esta materia é clave no módulo de Formación Obrigatoria Avanzada porque completa o estudo da Química Analítica impartido no Grado en Química.

Study programme competencies

Code	Study programme competences
A1	Define concepts, principles, theories and specialized facts of different areas of chemistry.
A2	Suggest alternatives for solving complex chemical problems related to the different areas of chemistry.
A4	Innovate in the methods of synthesis and chemical analysis related to the different areas of chemistry
B1	Possess knowledge and understanding to provide a basis or opportunity for originality in developing and / or applying ideas, often within a research context
B2	Students should apply their knowledge and ability to solve problems in new or unfamiliar environments within broader (or multidisciplinary) contexts related to their field of study.
B4	Students should be able to communicate their conclusions, and the knowledge and the reasons that support them to specialists and non-specialists in a clear and unambiguous manner
B5	Students must possess learning skills to allow them to continue studying in a way that will have to be largely self-directed or autonomous.
B7	Identify information from scientific literature by using appropriate channels and integrate such information to raise and contextualize a research topic
B10	Use of scientific terminology in English to explain the experimental results in the context of the chemical profession
B11	Apply correctly the new technologies to gather and organize the information to solve problems in the professional activity.

Learning aims

Learning outcomes	Study programme competences
Acquire a complete and integrated training of analytical methods used throughout the analytical process including the study of methods for sampling, sample preparation, determination of analytes, and processing and interpretation of results.	AC1	BC1 BC2 BC5 BC10
Overview of analytical methods and their selection and application to solving real problems.	AC2 AC4	BC4 BC7 BC11

Contents

Topic	Sub-topic
Topic 1	Trends in Analytical Chemistry.
Topic 2	Automation and miniaturization in Analytical Chemistry
Topic 3	Optimization and validation of analytical methods through chemometrics.

Planning

Methodologies / tests	Competencies	Ordinary class hours	Student’s personal work hours	Total hours
Guest lecture / keynote speech	A1 B1 B5 B10	16	24	40
Seminar	A2 A4 B2 B4 B7 B11	5	15	20
Supervised projects	A2 B1 B2 B4 B7 B11	3	9	12
Mixed objective/subjective test	A1 A2 B1 B2 B4	2	0	2

Personalized attention		1	0	1

(*)The information in the planning table is for guidance only and does not take into account the heterogeneity of the students.

Methodologies

Methodologies	Description
Guest lecture / keynote speech	The teacher will present the fundamental contents of each of the topics. For better learning, students will have teaching materials suitable for your personal preparation. All students can consult the teacher any aspect of the matter in the tutorial schedule established for this purpose. He taught in face classes.
Seminar	In the seminars the teacher will be clarified some issues addressed in the classroom, especially related to the practical application of the methodologies used. Students must work with scientific papers in English, with regulations, reports, etc. from which they must to extract and interpret information required for discussion in the classroom sessions.
Supervised projects	Students should develop, deliver and present work and in the corresponding session as presented and discussed about it. Students who have particular difficulty with the contents should contact the teacher to receive the necessary support. They are sessions. He taught in face classes.
Mixed objective/subjective test	A final exam will be done to assess the degree of learning both the theoretical and practical.

Personalized attention

Methodologies

Supervised projects

Seminar

Description

Throughout the course the teacher resolves any doubts on the subject that the student needs.
Students with recognition of part-time dedication and academic assistance waiver regime will be treated in tutoring (by appointment)

Assessment

Methodologies	Competencies	Description	Qualification
Supervised projects	A2 B1 B2 B4 B7 B11	guided academic activities and exposure are evaluated.	30
Mixed objective/subjective test	A1 A2 B1 B2 B4	This test will consist of theoretical questions and problems to assess the degree of learning from the contents of the subject.	55
Guest lecture / keynote speech	A1 B1 B5 B10	student participation is valued in the classroom	5
Seminar	A2 A4 B2 B4 B7 B11	work and active student participation is valued	10

Assessment comments
-The student will obtain the qualification of not submitted when don`t make the supervised project and not presented to the mixed test. As regards the successive academic years, the teaching-learning process, including continuous assessment, refers to an academic course and, therefore, would comezar a new course, including all activities and procedures the Assessment that is scheduled for that course. For students with part-time dedication and academic assistance waiver regime. in the event that the student can not perform all activities or continuous assessment tests, the teacher take appropriate measures to avoid prejudicing their qualification.

Sources of information

Basic	R. Kellner, J. M. Mermet, M. Otto, M. Valcarcel y H. M. Widmer, Eds (2004). “Analytical Chemistry: A Modern Approach to Analytical Science“. Ed. Wiley-VCH

Complementary	Valcárcel M., Cárdenas M.S (2000). Automatización y Miniaturización en Química Analític. Ed. Springer. Miller J.C., Miller J.N. (2002). Estadística y Quimiometría para Química Analítica. 2ª Ed. Prentice Hall. Madrid. Massart D.L., Vandegiste B.G.M., Buydens L.M.C., De Jong S., Lewi P.J., Smeyers-Verbeke, J. (1997). Handbook of chemometrics and qualimetrics. Part A.. Elsevier Science. Amsterdam Ramis Ramos G., García Álvarez-Coque M.C. (2001). Quimiometría. Síntesis. Madrid.

Recommendations

Subjects that it is recommended to have taken before

Subjects that are recommended to be taken simultaneously

Subjects that continue the syllabus

Other comments

(*)The teaching guide is the document in which the URV publishes the information about all its courses. It is a public document and cannot be modified. Only in exceptional cases can it be revised by the competent agent or duly revised so that it is in line with current legislation.