Identifying Data 2016/17
Subject (*) Deseño e Desenvolvemento de Materiais Avanzados Code 610509018
Study programme
Mestrado en Investigación Química e Química Industrial (plan 2016)
Descriptors Cycle Period Year Type Credits
Official Master's Degree Yearly
First Optativa 3
Language
Spanish
Teaching method Face-to-face
Prerequisites
Department Química Fundamental
Coordinador
Señaris Rodriguez, Maria Antonia
E-mail
m.senaris.rodriguez@udc.es
Lecturers
Señaris Rodriguez, Maria Antonia
E-mail
m.senaris.rodriguez@udc.es
Web
General description Esta asignatura pertence ao módulo da especialidade “Nanoquímica e Novos Materiais”, que engloba 4 asignaturas, todas elas intimamente relacionadas:
1.-Deseño e desenvolvemento de materiais avanzados
2.-Técnicas de caracterización de materiais
3.-Propiedades de materiais
4.-Materiais moleculares
Esta asignatura é clave no dito módulo para comprender qué son os materialis avanzados, que se espera deles á vista das súas propiedades e cales son as estratexias para o seu deseño e desenvolvemento.

Study programme competencies
Code Study programme competences
A1 Define concepts, principles, theories and specialized facts of different areas of chemistry.
A3 Apply materials and biomolecules in innovative fields of industry and chemical engineering.
A4 Innovate in the methods of synthesis and chemical analysis related to the different areas of chemistry
B1 Possess knowledge and understanding to provide a basis or opportunity for originality in developing and / or applying ideas, often within a research context
B4 Students should be able to communicate their conclusions, and the knowledge and the reasons that support them to specialists and non-specialists in a clear and unambiguous manner
B5 Students must possess learning skills to allow them to continue studying in a way that will have to be largely self-directed or autonomous.
B7 Identify information from scientific literature by using appropriate channels and integrate such information to raise and contextualize a research topic
B10 Use of scientific terminology in English to explain the experimental results in the context of the chemical profession
B11 Apply correctly the new technologies to gather and organize the information to solve problems in the professional activity.

Learning aims
Learning outcomes Study programme competences
- The student will learn the main strategies for the design and development of advanced materials. -The student will obtain an overview of the main advances in the development of different types of materials (ionic conductors, dielectrics, ferroelectrics, multiferroics, superconductors , semiconductors, optic materials, catalytic materials , magnetic materials , etc.) aand their applications in technological devices. - The student will understand composition-structure-microstruture- properties relationships - The student will understand the importance of nanomaterials for the development of new materials , and their role in the improvement of devices as well as their advantages as compared to conventional macrosacopic materials AC1
AC3
AC4
BC1
BC4
BC5
BC7
BC10
BC11

Contents
Topic Sub-topic
I.Introduction to Nanochemistry and general Introduction to synthesis of materials -Introduction to Nanochemistry. Surface/volume ratio. Nanomanipulation.
- General Introduction to synthesis of materials.
Top-Down and Bottom-Up methods
Growth of Single crystals
Preparation of polycrystalline materials: Ceramic method vs alternative methods (decomposition of nitrates, coprecipitation, sol-gel, high pressure synthesis , microwave synthesis).
II. Nanomaterials
Metallic, semiconducting and magnetic nanomaterials
Synnthesis. Size, shape and surrounding effects
Applications.
III. Surface modification of nanomaterials.
Surface modification of nanomaterials.
Ligand exchange. Layer by layer method
Organic and inorganic coatings
IV. Overview of different outstanding non-molecular materials I: Transition metal oxides Overview of transition metal oxides with emphasis in mixed oxides.
Synthesis, structure, properties and main applications
Theme 5.
Overview of different outstanding non-molecular materials II: zeolites, Inorganic-organic hybrids (MOFs) , etc.
-Inorganic-organic hybrids (MOFs): Synthesis, structure, properties and main applications.
-Zeolites: Synthesis, structure, properties and main applications.

Planning
Methodologies / tests Competencies Ordinary class hours Student’s personal work hours Total hours
Guest lecture / keynote speech A1 A3 A4 B5 12 0 12
Seminar B4 B7 B10 7 0 7
Document analysis B5 B7 B11 0 12 12
Problem solving A3 A4 B1 B4 B5 0 24 24
Objective test A1 A3 A4 B1 B4 B5 B7 B10 B11 1 18 19
 
Personalized attention 1 0 1
 
(*)The information in the planning table is for guidance only and does not take into account the heterogeneity of the students.

Methodologies
Methodologies Description
Guest lecture / keynote speech Magisterial lessons (with the use of blackboard and computer), complemented with the tools of virtual teaching
Seminar Practical seminars conducted by teachers of the Master, or invited professionals from companies, the Administration or other universities. Interactive sessions related to the subjects with discussions and exchange of points of view with the students
Document analysis Personal study based on different sources of information.
Problem solving Resolution of practical exercises (problems, quizzes, processing and interpretation of information, evaluation of scientific publications, etc.).
Objective test Preparation of the different tests for verification of obtaining both theoretical and practical knowledges, and the acquisition of skills and attitudes.

Personalized attention
Methodologies
Seminar
Document analysis
Problem solving
Description
Individual or small group tutoring.

Assessment
Methodologies Competencies Description Qualification
Guest lecture / keynote speech A1 A3 A4 B5 GUEST LECTURE + SEMINARS + PROBLEM SOLVING: 25% of global qualification 0
Seminar B4 B7 B10 GUEST LECTURE + SEMINARS + PROBLEM SOLVING: 25% of global qualification 0
Problem solving A3 A4 B1 B4 B5 GUEST LECTURE + SEMINARS + PROBLEM SOLVING: 25% of global qualification 25
Objective test A1 A3 A4 B1 B4 B5 B7 B10 B11 5% of global qualification 75
 
Assessment comments

1. Assessment procedure. The
assessment of this subject will be done through a system whose sections and
their respective weighting is detailed:

Assessment system (Weighting):

- Final examination (75%)

- Continuous evaluation (25%)
through:

-- problems solving and case
studies and

-- continuous evaluation of the
student by means of written and oral questions during the course and eventual
oral presentation of papers and reports.

According to this, the final
exam will have a weight of 75% in the qualification of the subject.
Continuous evaluation will have a 25% weight in the qualification of the
subject. The student score is obtained as a result of applying the following
formula:

Final score = 0.75 x N1 + 0.25
x N2

being N2 and N1 the numerical
scores of the corresponding continuous assessment (scale 0-10) and the final
examination (scale 0-10), respectively. Face-to-face teaching activities
(seminars and tutorials) are compulsory. Repeater students will have the same
regime of classes to those who are studying the subject for the first time.

2. Recommendations with regard
to the evaluation.

The student should review the
theoretical concepts introduced in the various topics using the supporting
material provided by teachers and the literature recommended for each theme.
The degree of success in the resolution of the exercises provides a measure
of the student's preparation to deal with the final examination of the
subject. Students who find difficulties in working the proposed activities
should consult with the teacher, with the goal that it can analyze the
problem and help solve these challenges.

3. Recommendations with regard
to the recovery.

Teacher will discuss with
students who do not successfully overcome the evaluation process, and want
it, the difficulties encountered in learning the contents of the subject. The
teacher will also provide additional material (questions, exercises, exams,
etc.) to reinforce the learning of the subject.

4. Others.

Attendance at face-to-face
activities (face to face lectures, seminars and tutorials) is mandatory. The
faults must be documentary supported, accepting reasons referred to in the
University regulations.


Sources of information
Basic

1. A.R. West: "Solid State Chemistry and its Applications". Wiley, 2 ed., 2014

2. C. N. R. Rao, Chintamani Nagesa Ramachandra Rao “New Directions in Solid State Chemistry”. 2nd edition, Cambridge University Press, 1997

3. C.N. R. Rao and B. Raveau, “Transition metal oxides”, John Wiley & Sons ,1998.

4. P. Gómez-Romero, C. Sanchez “Functional Hybrid Materials” (eds.), Wiley-VCH, 2003,

5. G. A. Ozin, Nanochemistry: A Chemical Approach to Nanomaterials, , 2005

6. Gunter Schmid, Clusters and colloids : from theory to applications, , 1994

2. D.L. Feldheim, C.A. Foss Jr., Metal Nanoparticles, , 2001

3. G. Schmid, Nanoparticles. From Theory to Application, , 2004

4. Brongersma, M. L.; Kik, P. G. Surafce plasmon nanophotonics, Springer, 2007.

5. Shalaev, V. M.; Kawata, S. Nanophotonics with surface plasmons, Elsevier, 2007.

7. G. Cao: "Nanostructures and Nanomaterials: Syntesis, Properties and Applications". Imperial College Press, 2004.

8. U. Schubert, N. Hüsing: "Synthesis of Inorganic Materials". Wiley-VCH, 2 ed., 2004.

9. K. T. Ramesh: "Nanomaterials: Mechanics and Mechanisms", Springer-Verlag, 2009.

10. D. Vollath: "Nanomaterials : an introduction to synthesis, properties and applications". Weinheim, Wiley-VCH, 2013.

11. Kenneth J. Klabunde (Ed.): “Nanoscale materials in chemistry”. Wiley-Interscience, New York, 2001.

12. J.A. Schwarz, C.I. Contescu, K. Putyera (Editores): "Dekker Encyclopedia of nanoscience and nanotechnology" (5 volumes). Marcel Dekker, 2004.

13. M. Lazzari, G. Liu, S. Lecommandoux (Editores): “Block Copolymers in Nanoscience”. Wiley-VCH, 2006.

14. L. C. Sawyer, D. T. Grubb, G. F. Meyers (Editores): “Polymer Microscopy” Springer, 2008.

15. V. Rotello, S. Thayumanavan (Editores) “Molecular Recognition and Polymers”

Además se recomendarán para cada tema textos complementarios (artículos, páginas web, textos específicos) en el momento de impartición de la asignatura.

Complementary


Recommendations
Subjects that it is recommended to have taken before

Subjects that are recommended to be taken simultaneously
Propiedades de Materiais/610509020
Técnicas de Preparación e Caracterización de Materiais/610509019

Subjects that continue the syllabus

Other comments

In this module it is essential to make a global approach to materials, trying to understand the close relationship that exists between the different materials synthetic procedures and their structural and microstructural characteristics, with their properties and, therefore, with their applications.



(*)The teaching guide is the document in which the URV publishes the information about all its courses. It is a public document and cannot be modified. Only in exceptional cases can it be revised by the competent agent or duly revised so that it is in line with current legislation.