Identifying Data 2019/20
Subject (*) Selection and validation of Analytical methodologies Code 610509101
Study programme
Mestrado Universitario en Investigación Química e Química Industrial (Plan 2017)
Descriptors Cycle Period Year Type Credits
Official Master's Degree Yearly
First Obligatory 3
Language
Spanish
Teaching method Face-to-face
Prerequisites
Department Química
Coordinador
Muniategui Lorenzo, Soledad
E-mail
soledad.muniategui@udc.es
Lecturers
Carlosena Zubieta, Alatzne
Muniategui Lorenzo, Soledad
E-mail
alatzne.carlosena@udc.es
soledad.muniategui@udc.es
Web http://http://www.usc.es/gl/centros/quimica/curso/master.html
General description Esta materia ten por obxeto dar ao estudante o coñecemento dos principios básicos para as boas prácticas na medición analítica, facendo fincapé na importancia de empregar métodos validados. Dar unha orientación sobre a avaliación dos métodos de análisis na súa adecuación ao uso con diferentes guías de validación, de carácter xeral ou máis específico. Introducir ao alumno en técnicas innovadoras de análisis, de interese no campo industrial e da investigación. Desenvolver no alumno a súa capacidade para resolver problemas reais de casos prácticos de análisis de interese clínico, ambiental, entre outros.

Study programme competencies
Code Study programme competences
A1 Define concepts, principles, theories and specialized facts of different areas of chemistry.
A3 Innovate in the methods of synthesis and chemical analysis related to the different areas of chemistry
A5 Properly assess risks and environmental and socioeconomic impacts associated with special chemicals
A6 Design processes involving the treatment or disposal of hazardous chemicals
A7 Operate with advanced instrumentation for chemical analysis and structural determination.
A8 Analyze and use the data obtained independently in complex laboratory experiments and relating them with the chemical, physical or biological appropriate techniques, including the use of primary literature sources
A9 Promote innovation and entrepreneurship in the chemical industry and in research.
B2 Students should apply their knowledge and ability to solve problems in new or unfamiliar environments within broader (or multidisciplinary) contexts related to their field of study.
B3 Students should be able to integrate knowledge and handle complexity, and formulate judgments based on information that was incomplete or limited, include reflecting on social and ethical responsibilities linked to the application of their knowledge and judgments.
B4 Students should be able to communicate their conclusions, and the knowledge and the reasons that support them to specialists and non-specialists in a clear and unambiguous manner
B5 Students must possess learning skills to allow them to continue studying in a way that will have to be largely self-directed or autonomous.
B10 Use of scientific terminology in English to explain the experimental results in the context of the chemical profession
B11 Apply correctly the new technologies to gather and organize the information to solve problems in the professional activity.
B12 Being able to work in a team and adapt to multidisciplinary teams.
C1 CT1 - Elaborar, escribir e defender publicamente informes de carácter científico e técnico
C2 CT2 - Traballar en equipo e adaptarse a equipos multidisciplinares.
C3 CT3 - Traballar con autonomía e eficiencia na práctica diaria da investigación ou da actividade profesional.
C4 CT4 - Apreciar o valor da calidade e mellora continua, actuando con rigor, responsabilidade e ética profesional.

Learning aims
Learning outcomes Study programme competences
To know how to select and implement best practice measurement and analytical experimentation, ensuring the quality of the chemical data through the validation of the analytical methodologies. AC8
AC9
BC3
BC4
BC5
CC1
CC4
To know advanced techniques of sampling, sample treatment and instrumental determination in environmental analysis AC5
AC6
AC7
AC9
CC1
To know how to analyze and solve chemical problems related to the environment based on analytical criteria. Planning and implementation of the stages of an analytical process AC1
AC3
BC2
BC10
BC11
BC12
CC2
CC3

Contents
Topic Sub-topic
Item 1. Selection of analytical methodologies
Item 2. Implementation, validation and verification of chemical analysis methods.
Item 3. Innovative Technologies in Analytical Chemistry.
Case Studies

Planning
Methodologies / tests Competencies Ordinary class hours Student’s personal work hours Total hours
Seminar A9 B2 B11 C2 C4 3 9 12
Supervised projects A5 B3 B4 B5 B10 B12 C1 C3 2 18 20
Mixed objective/subjective test A1 A8 B2 C1 3 0 3
Laboratory practice A3 A5 A6 A7 A8 A9 5 5 10
Guest lecture / keynote speech A9 B3 B12 C4 10 20 30
 
Personalized attention 0 0 0
 
(*)The information in the planning table is for guidance only and does not take into account the heterogeneity of the students.

Methodologies
Methodologies Description
Seminar Seminars clarify and extend some aspects covered in lectures and laboratory practice, especially related to the practical application of the studied methodologies. Students participate and discuss possible strategies to solve industrial and environmental problems under the teacher guidance
Supervised projects Supervised projects will include finding information from different sources, presentation and oral defense of a topic proposed by the teacher related to any environmental, industrial, etc problem
Mixed objective/subjective test A final exam will be done to assess the degree of learning both the theoretical and practica
Laboratory practice In the lab sessions the student will perform the application of theoretical concepts studied throughout the course and will also it will contact advanced technical and analytical instrumentation.
Guest lecture / keynote speech Teacher explains the fundamental concepts and the most important contents of each subject. It also proposes different issues that should be discussed and resolved by the students, encouraging participation

Personalized attention
Methodologies
Seminar
Supervised projects
Description
Throughout the course the teacher resolves any doubts on the subject that the student needs.
In seminars and supervised projects, the teacher supervises the methodology used to solve the proposed problems, solves the student´s doubts and guides the learning process.

Students with recognition of part-time dedication and academic assistance waiver regime will be treated in tutoring (by appointment)

Assessment
Methodologies Competencies Description Qualification
Seminar A9 B2 B11 C2 C4 Work and active participation of students will be evaluated 5
Supervised projects A5 B3 B4 B5 B10 B12 C1 C3 The academic activities will be evaluated by performing and oral defense of the supervised activities 30
Mixed objective/subjective test A1 A8 B2 C1 Learning degree for the course contents and skill acquisition by students will be assessed through an objective test. It will consist of theoretical questions and applied problems 60
Laboratory practice A3 A5 A6 A7 A8 A9 Practice work and active participation of students will be evaluated on a continuing process. 5
 
Assessment comments
To pass the subject, students must regulary attendance at all evaluable activities and to attain a minimum cualification in each of them. The student will obtain the qualification of No Presented they do not perform the mentored work and not present the final exam. The scores for the activities will remain in the July, except for the mixed test which shall be repeated in case of being suspended.

The
following academic courses, the teaching-learning process, including
all evaluable activities, return to start a new course.
For
students with a part-time dedication and academic assistance waiver regime, in the event that they can not perform all activities or continuous assessment test, the teacher will
take appropriate action to avoid prejudicing their qualification.

Sources of information
Basic R. Kellner, J. M. Mermet, M. Otto, M. Valcarcel y H. M. Widmer, (2004). Básica. Eds. “Analytical Chemistry: A Modern Approach to Analytical Science. Wiley-VCH
Eurolab España. P.P. Morillas y colaboradores (2016). Guía Eurachem: La adecuación al uso de los métodos analíticos – Una Guía de laboratorio para la validación de métodos y temas relacionados . Disponible en www.eurachem.org
M. Valcárcel (1999). Principios de Química Analítica. Springer, Barcelona

Complementary Valcárcel M., Cárdenas M.S (2000.). Automatización y Miniat urización en Química Analítica. Ed. Springer.
Compañó Beltrán R., Rios Castro A (2002). Garantía de calidad en los laboratorios analíticos. Síntesis. Madrid.
Ramis Ramos G., García Álvarez-Coque M.C (2001). Quimiometría. Síntesis. Madrid.
Kruve A. et al. (2015). Tutorial review on validation of liquid chromato graphy–mass spectrometry methods: Part I. Analytica Chimica Act a 870 (2015) 8–28
Kruve A. et al. (). Tutorial review on validation of liquid chromato graphy–mass spectrometry methods: Part II. Analytica Chimica Act a 870 (2015) 29–44
I. Rodríguez, E. Trullos, X. Rius (2003). Validación de Métodos Analíticos Cualitativos. Técnicas de Laboratorio, 281 (2003) 328-335. http:/www.quimica.urv.es/quimio


Recommendations
Subjects that it is recommended to have taken before

Subjects that are recommended to be taken simultaneously

Subjects that continue the syllabus

Other comments
Students must review the theoretical concepts introduced in different topics using the recommended bibliography. Those students who encounter significant difficulties in working the proposed activities must go in the tutorial hours of teachers, in order to be able to analyze the problem and try to solve those difficulties.


(*)The teaching guide is the document in which the URV publishes the information about all its courses. It is a public document and cannot be modified. Only in exceptional cases can it be revised by the competent agent or duly revised so that it is in line with current legislation.