To pass the subject two basic requirements are needed:
1.- The realization of laboratory practice is mandatory to pass the subject.

2.-Reach a minimum qualification in the laboratory practice and in each mixed test. This minimum qualification will cannot be lower than 5 (over 10). Note that the subject will not be approved (even when the overall sum exceeds 5) if one of these particular scores do not reach 5. In this case, the subject is failed and the final qualification will be 4.5.

In the first and second opportunity, the students who carried out the laboratory practice but the obtained qualification was lower than 5, will have the opportunity to, in addition to the mixed test, perform a specific test related to the laboratory practice. The score of this test will replaced the grade obtained in practice for the overall rating.

Students who do not participate on the problem solving and supervised projects, and do not carry out the short answer questions will score 0 in these sections.

The student will obtain the qualification of No Presented when the student does not assist to the laboratory practice and neither attend to the mixed test.

In the context of "continuous evaluation" the "second opportunity" is a second opportunity of realisation of the mixed test and a specific test related to the laboratory practice. Therefore, the laboratory practice (except for students who did not get a minimum of 5), problem solving, supervised projects and short answer questions will keep the qualifications obtained along the course, whereas the qualification of the mixed test and a specific test related to the laboratory practice corresponding to second opportunity will substitute to those obtained in the first opportunity.

The students evaluated in the "second opportunity" only will be able to opt to Mark Honor if the maximum number of the Honors for the corresponding course has not covered in its whole in the "first opportunity".

For students with recognition of a part-time dedication, the evaluation will be carried out under the same criteria.

For students with academic exemption waiver assistance, conducting laboratory practices is mandatory and they will be provided within the flexibility to allow coordinating schedules and material and human resources. On the other hand, assistance to the greatest number of problem solving sessions will be provided; if students can not attend the problem solving sessions, they will make a mentored work. Therefore, these students will be evaluated by the qualifications obtained in laboratory practice (20%), in the mixed test (55%), in short answer questions (10%), in the activities of the problem solving sessions(10%)and supervised projects (5%). This will be applied to both opportunities.

Learning outcomes	Study programme competences
To apply the foundations of the chemical equilibria in the classical methods of analysis	A4 A7 A16 A24	B1 B2 B4	C1 C6
To learn the data handling and present the analytical results	A7 A16 A20	B1 B2 B4	C1
To understand the qualitative and quantitative aspects of the analysis	A4 A7 A20 A21 A24	B1 B2 B4	C1 C6
To acquire the basic skill in the laboratory of Analytical Chemistry (basic operations of the classical chemical analysis)	A7 A16 A17 A19 A20 A21 A23 A24	B1 B2 B3 B4 B5	C1 C6

Topic	Sub-topic
Chapter 1: Analytical Chemistry	Definition and scopes Qualitative and quantitative analysis The analytical process Classification of methods and techniques
Chapter 2: Titrimetric Methods	Basic concepts, titrimetric reaction and types of Titrations Primary standards, standard solutions and standardized solutions Equivalence point and detection of the end point Titration curves Errors associated to titrimetric methods
Chapter 3: Acid-Base Titrations	Acid-Base titration theory. Titration curves Indicators for acid-base titrations. Selection of an indicator Strong acid versus strong base and vice versa Weak acid versus strong base and vice versa Titration of polyprotic acids or bases and their salts Titration of mixtures of acids or bases Acid-Base titration in nonaqueous solvents Applications
Chapter 4: Redox Titrations	Titration curves Redox indicators and their selection Oxidizing and reducing agents used prior to titration Titrations with oxidizing agents Titrations with reducing agents Determination of organic and inorganic compounds
Chapter 5: Complexometric Titrations	Coordination compounds of interest in titrimetric analysis Titration curves and the factors that affect them Metal ion indicators for chelometric titrations Titrations with polyaminocarboxylic acids
Chapter 6: Precipitation Titrations	Precipitation reactions of interest in titrimetric analysis Titration curves Titration of mixtures Detection of the end point: Mohr, Volhard and Fajans methods
Chapter 7: Gravimetric Analysis	Principles of the gravimetric analysis Steps and classification of gravimetric methods Precipitation process. Conditions for analytical precipitation Gravimetry by chemical precipitation. Treatment of precipitates Gravimetry by volatilization and absortion Gravimetric calculations
Chapter 8: Evaluation of Analytical Data	Definitions and basic concepts Statistic treatment for indeterminated errors The confidence limit Rejection of a result Tests of significance Analytical data how present them
Chapter 9: Qualitative Analysis	Application of chemical reactions to the qualitative analysis Analytical characteristics of chemical reactions (sensitivity, selectivity and safety) General and specific reagents Analytical characteristics and reagents for metal ions Analytical characteristics and reagents for anions
Module: Laboratory practice	Acid-Base Titrations Redox Titrations Complexometric Titrations Precipitation Titrations Gravimetric Analysis Evaluation of Analytical Data

Methodologies / tests	Competencies	Ordinary class hours	Student’s personal work hours	Total hours
Guest lecture / keynote speech	A4 A7 A21 B1	24	36	60
Problem solving	A7 A16 A20 B1 B2 B4 C1	8	18	26
Seminar	A7 A20	2	0	2
Laboratory practice	A7 A16 A17 A19 A20 A21 A23 A24 B1 B2 B3 B4 B5 C1 C6	18	18	36
Short answer questions	A4 A7 A21 B4	0	1.5	1.5
Supervised projects	A7 A16 A20 B1 B2 B4 C1	0	3	3
Mixed objective/subjective test	A4 A7 A20 A21 A24 B1 B2 C1 C6	3	18	21

Personalized attention		0.5	0	0.5

(*)The information in the planning table is for guidance only and does not take into account the heterogeneity of the students.

Methodologies	Description
Guest lecture / keynote speech	In the lecture classes the professor will develop the fundamental contents of the program of the subject. To make a good use of these sessions, the student will have to prepare previously the fundamental appearances of the topic to treat, employing the educational material (diagram that reflects the contents of each topic), which will be provided to the student through the Moodle platform. The student also will must read the chapter regarding to the topic to treat in the recommended bibliography
Problem solving	Classes in small groups conceived like a group of activities in which the student must participate on a direct way. They are devoted to the resolution of the bulletins of problems, which previously will have been provided to the student through the Moodle platform, and that the students will have to realise of autonomous form for discussion in these classes. Besides, in these sessions any doubts on any appearance related with the lecture sessions will be resolved.
Seminar	Initial activity, before beginning the laboratory sessions, which consists on 1 session of 2 hours. In this session, the students will be exposed to the educational methodology that will be employed in the practices of laboratory.
Laboratory practice	6 laboratory sessions of 3 hours of length, in which the student will carry out the application of the theoretical concepts studied in the classroom. Each practice owns a script and a prelaboratory exercise which will be provided to the student (through Moodle) previously to the practice sessions. The realisation of the prelaboratory exercises before starting the laboratory practice is mandatory. The scripts will have questions that the students will have to answer and deliver once finished the practices. During laboratory sessions, and on a simultaneous way to the realisation of the experiments, the student will have to elaborate a fascicle of laboratory that collect the calculations and the experimental procedures. The professor will review the notebook of each student in each laboratory session.
Short answer questions	Exams about the topics of the subject will be carried out employing short answer questions . These exams will be realised employing the Moodle platform.
Supervised projects	Siupervised learning process in small groups (3-4 students) with the aim of helping students to work independently and encouraging students to become responsible for their own learning. The proposed activities will be related with problem solving sessions. The students will work together to solve the tasks assigned by the teacher, with the aim of optimising their learning experience and that of other members of group. The activities will be discussed in a tutelage session.
Mixed objective/subjective test	Two written exams will be carried out in each one of the two official announcements of January/July. One of them will evaluate the learning of the student by means of questions of theory and applied theory and the other one will consist on the resolution of problems.

Methodologies	Competencies	Description	Qualification
Laboratory practice	A7 A16 A17 A19 A20 A21 A23 A24 B1 B2 B3 B4 B5 C1 C6	It will be evaluated the suitable realisation of the prelaboratory exercises, the skill in the realisation of the experimental work, the interpretation of the data obtained, as well as the correct realisation of the calculations, the answers to the questions of practices (that they will have to deliver) and the preparation of the notebook of laboratory.	20
Problem solving	A7 A16 A20 B1 B2 B4 C1	The work carried out before and during the sessions as well as the actitude and degree of participation of the student in the classes.	10
Mixed objective/subjective test	A4 A7 A20 A21 A24 B1 B2 C1 C6	Two written exams in each one of the two official announcements of January/July: one of them will consist on questions of theory and applied theory and the another one will consist on exercises focused to the resolution of problems.	55
Supervised projects	A7 A16 A20 B1 B2 B4 C1	The adequate resolution of the proposed projects, the degree of participation of the student in the tutelage session, and the quality of explanation of each activity.	5
Short answer questions	A4 A7 A21 B4	Exams to be realised through the Moodle platform about the topics of the subject by means of short answer questions.	10

Assessment comments
To pass the subject two basic requirements are needed: 1.- The realization of laboratory practice is mandatory to pass the subject. 2.-Reach a minimum qualification in the laboratory practice and in each mixed test. This minimum qualification will cannot be lower than 5 (over 10). Note that the subject will not be approved (even when the overall sum exceeds 5) if one of these particular scores do not reach 5. In this case, the subject is failed and the final qualification will be 4.5. In the first and second opportunity, the students who carried out the laboratory practice but the obtained qualification was lower than 5, will have the opportunity to, in addition to the mixed test, perform a specific test related to the laboratory practice. The score of this test will replaced the grade obtained in practice for the overall rating. Students who do not participate on the problem solving and supervised projects, and do not carry out the short answer questions will score 0 in these sections. The student will obtain the qualification of No Presented when the student does not assist to the laboratory practice and neither attend to the mixed test. In the context of "continuous evaluation" the "second opportunity" is a second opportunity of realisation of the mixed test and a specific test related to the laboratory practice. Therefore, the laboratory practice (except for students who did not get a minimum of 5), problem solving, supervised projects and short answer questions will keep the qualifications obtained along the course, whereas the qualification of the mixed test and a specific test related to the laboratory practice corresponding to second opportunity will substitute to those obtained in the first opportunity. The students evaluated in the "second opportunity" only will be able to opt to Mark Honor if the maximum number of the Honors for the corresponding course has not covered in its whole in the "first opportunity". For students with recognition of a part-time dedication, the evaluation will be carried out under the same criteria. For students with academic exemption waiver assistance, conducting laboratory practices is mandatory and they will be provided within the flexibility to allow coordinating schedules and material and human resources. On the other hand, assistance to the greatest number of problem solving sessions will be provided; if students can not attend the problem solving sessions, they will make a mentored work. Therefore, these students will be evaluated by the qualifications obtained in laboratory practice (20%), in the mixed test (55%), in short answer questions (10%), in the activities of the problem solving sessions(10%)and supervised projects (5%). This will be applied to both opportunities.

Basic	HARRIS, DANIEL C (2007). Análisis Químico Cuantitativo . Barcelona, Ed. Reverté SKOOG D.A., WEST D.M., HOLLER F.J. y CROUCH S.R. (2005). Fundamentos de Química Analítica . Madrid, Ed. Paraninfo SKOOG D. A., WEST D.M. y HOLLER F. J (1997). Fundamentos de Química Analítica . Barcelona, Ed. Reverté
	The book "Análisis Químico Cuantitativo" of the author Daniel C. Harris (Ed. Reverté SA), is available in the UDC library web page.
Complementary	GUITERAS J. RUBIO R. y FONRODONA G. (2003 ). Curso Experimental en Química Analítica . Madrid, Ed. Síntesis SILVA M. y BARBOSA J. (2002 ). Equilibrios iónicos y sus Aplicaciones Analíticas . Madrid, Ed. Síntesis LÓPEZ CANCIO J.A. (2005). Problemas Resueltos de Química Analítica . Madrid, Ed. Paraninfo YÁÑEZ-SEDEÑO P., PINGARRÓN J.M. y MANUEL DE VILLENA F.J. (2003 ). Problemas Resueltos de Química Analítica . Madrid, Ed. Síntesis BURRIEL MARTI F., LUCENA CONDE F., ARRIBAS JIMENO S. y HERNÁNDEZ MÉNDEZ J. (2001 ). Química Analítica Cualitativa . Madrid, Ed. Paraninfo HARVEY D. (2002). Química Analítica Moderna . Madrid, Ed. McGraw-Hill

Other comments
To register on this subject it is recommended having passed the subject “Chemical 3”