Identifying Data 2022/23
Subject (*) Techniques of Characterisation of Nanomaterials 2 Code 610G04030
Study programme
Grao en Nanociencia e Nanotecnoloxía
Descriptors Cycle Period Year Type Credits
Graduate 2nd four-month period
Third Obligatory 6
Language
Spanish
Galician
Teaching method Face-to-face
Prerequisites
Department Enxeñaría Naval e Industrial
Física e Ciencias da Terra
Química
Coordinador
Fernandez Perez, Maria Isabel
E-mail
isabel.fernandez.perez@udc.es
Lecturers
Andrade Garda, Jose Manuel
Canle López, Moisés
Fernandez Perez, Maria Isabel
Garcia Dopico, Maria Victoria
Montero Rodríguez, María Belén
Santaballa Lopez, Juan Arturo
E-mail
jose.manuel.andrade@udc.es
moises.canle@udc.es
isabel.fernandez.perez@udc.es
victoria.gdopico@udc.es
belen.montero@udc.es
arturo.santaballa@udc.es
Web http://https://campusvirtual.udc.gal/my/
General description Descrición: Comprender os aspectos básicos das técnicas para a caracterización morfolóxica, estrutural e microestructural dos materiais, así como desenvolver criterios que permitan selección entre as técnicas de caracterización aquela que resulte máis apropiada á hora de resolver problemas concretos.

Contexto: A materia ofértase cando xa se cursaron outras materias que proporcionan coñecementos básicos sobre a interacción radiación-materia que servirán como inicio para o desenvolvemento desta materia.

Study programme competencies
Code Study programme competences
A1 CE1 - Comprender los conceptos, principios, teorías y hechos fundamentales relacionados con la Nanociencia y Nanotecnología.
A2 CE2 - Aplicar los conceptos, principios, teorías y hechos fundamentales relacionados con la Nanociencia y Nanotecnología a la resolución de problemas de naturaleza cuantitativa o cualitativa.
A4 CE4 - Desarrollar trabajos de síntesis y preparación, caracterización y estudio de las propiedades de materiales en la nanoescala.
A5 CE5 - Conocer los rasgos estructurales de los nanomateriales, incluyendo las principales técnicas para su identificación y caracterización
A6 CE6 - Manipular instrumentación y material propios de laboratorios para ensayos físicos, químicos y biológicos en el estudio y análisis de fenómenos en la nanoescala.
A7 CE7 - Interpretar los datos obtenidos mediante medidas experimentales y simulaciones, incluyendo el uso de herramientas informáticas, identificar su significado y relacionarlos con las teorías químicas, físicas o biológicas apropiadas.
A8 CE8 - Aplicar las normas generales de seguridad y funcionamiento de un laboratorio y las normativas específicas para la manipulación de la instrumentación y de los productos y nanomateriales.
A9 CE9 - Evaluar correctamente los riesgos sanitarios y de impacto ambiental asociados a la Nanociencia y la Nanotecnología.
B1 CB1 - Que los estudiantes hayan demostrado poseer y comprender conocimientos en un área de estudio que parte de la base de la educación secundaria general, y se suele encontrar a un nivel que, si bien se apoya en libros de texto avanzados, incluye también algunos aspectos que implican conocimientos procedentes de la vanguardia de su campo de estudio
B3 CB3 - Que los estudiantes tengan la capacidad de reunir e interpretar datos relevantes (normalmente dentro de su área de estudio) para emitir juicios que incluyan una reflexión sobre temas relevantes de índole social, científica o ética
B7 CG2 - Resolver problemas de forma efectiva.
B8 CG3 - Aplicar un pensamiento crítico, lógico y creativo.
B9 CG4 - Trabajar de forma autónoma con iniciativa.
B10 CG5 - Trabajar de forma colaborativa.
B11 CG6 - Comportarse con ética y responsabilidad social como ciudadano/a y como profesional.
C2 CT2 - Dominar la expresión y la comprensión de forma oral y escrita de un idioma extranjero
C6 CT6 - Adquirir habilidades para la vida y hábitos, rutinas y estilos de vida saludables
C7 CT7 - Desarrollar la capacidad de trabajar en equipos interdisciplinares o transdisciplinares, para ofrecer propuestas que contribuyan a un desarrollo sostenible ambiental, económico, político y social.
C8 CT8 - Valorar la importancia que tiene la investigación, la innovación y el desarrollo tecnológico en el avance socioeconómico y cultural de la sociedad
C9 CT9 - Tener la capacidad de gestionar tiempos y recursos: desarrollar planes, priorizar actividades, identificar las críticas, establecer plazos y cumplirlos

Learning aims
Learning outcomes Study programme competences
Deepen the understanding of the basic aspects of advanced techniques of morphological, structural and microstructural characterization of materials. A1
A2
B1
C2
Ability to correctly interpret the results obtained through different characterization techniques A5
A7
B3
B7
B8
B10
C2
C7
C8
Develop selection criteria among the characterization techniques for the resolution of specific problems. A4
A6
A8
A9
B7
B8
B9
B11
C6
C7
C8
C9

Contents
Topic Sub-topic
MODULE 1: Characterization using spectroscopies: • Ultraviolet-visible (UV-Vis)
• Diffuse reflectance (DRS)
• Infrared with Fourier transform (FT-IR)
• Raman
• Surface enhanced Raman spectroscopy. (SERS)
• X-ray spectroscopy
MODULE 2: Characterization using microscopies: • Atomic force microsopy
• Tunnel effect
• Confocal

Planning
Methodologies / tests Competencies Ordinary class hours Student’s personal work hours Total hours
Guest lecture / keynote speech A1 C2 5 11 16
Laboratory practice A2 A4 A5 A6 A7 A8 A9 B1 B3 B7 B8 B9 B10 B11 C6 C7 C8 C9 55 63 118
Oral presentation A1 A2 A7 B1 B3 B7 B8 B9 B10 B11 C2 C6 C7 C8 C9 2 8 10
Mixed objective/subjective test A1 A2 A4 A5 A7 A8 A9 B1 B3 B7 B8 B9 B11 C2 C6 C9 3 0 3
 
Personalized attention 3 0 3
 
(*)The information in the planning table is for guidance only and does not take into account the heterogeneity of the students.

Methodologies
Methodologies Description
Guest lecture / keynote speech Sesións previas onde se presentarán os distintos módulos da materia e introduciranse os conceptos necesarios para as diferentes técnicas experimentais.
Laboratory practice Laboratory practices and interpretation and analysis of experimental results.

The student must upload in the Moodle / Onenote of the subject the different activities carried out during the sessions (laboratory notebook, brief review, graphics, etc.) in order to evaluate the use of the work sessions.

A report will be delivered per module that will be written following the instructions of the teaching staff.
The report will be made individually and dates will be established for delivery through the virtual field.
Several dates will be established, within a group session, to expose individually the activities carried out during the practice sessions. The teacher will assign the activity.
Several dates will be established, within a group session, to expose individually the activities carried out during the practice sessions. The teacher will assign the activity.
Oral presentation Several dates will be established, within a group session, to expose individually the activities carried out during the practice sessions. The teacher will assign the activity
Mixed objective/subjective test Combination of different types of questions: type test, problems, short answer or essay which allows to evaluate the knowledge, reasoning capacity and critical spirit.

Personalized attention
Methodologies
Oral presentation
Description
To look for a deeper understanding of the subject content and to find the best personalized strategy in problem solving.
Tutoring schedule will be decided at lecturers and students convenience. They take place at the lecturers' offices


Assessment
Methodologies Competencies Description Qualification
Oral presentation A1 A2 A7 B1 B3 B7 B8 B9 B10 B11 C2 C6 C7 C8 C9 Avaliarase:
-a calidade da información contida a presentación, así como a habilidade mostrada.
-a capacidade para defender o traballo presentado.
15
Mixed objective/subjective test A1 A2 A4 A5 A7 A8 A9 B1 B3 B7 B8 B9 B11 C2 C6 C9 Exame final con dous partes, unha teórica (50%) que inclúe preguntas de tipo test, de resposta breve e/o de ensaio, e outra de resolución/análise de problemas (50%). 20
Laboratory practice A2 A4 A5 A6 A7 A8 A9 B1 B3 B7 B8 B9 B10 B11 C6 C7 C8 C9 Avaliarase:
-aspectos operacionales, planificación, organización e realización do caderno de laboratorio.
-preparación de gráficas, revisión bibliográfica, etc.
-elaboración de informes, o que inclúe a análise critico de resultados.
65
 
Assessment comments

Assistance at all the sessions is obligatory to be able to pass the subject.

The pass of the subject is obtained by obtaining a final grade of at least 5 points out of 10. The final grade is obtained according to the established percentages and the previously set restrictions.


First opportunity. At least a grade of 4 over ten in each of
the two parts of the final exam is required to take into consideration the rest
of the assessable activities. The final grade is obtained according to
the established percentages and the previously set restrictions
Second opportunity. Repetition of the mixed test. The final
grade is obtained according to the established percentages and the previously
set restrictions

In both oportunities, in spite of getting
a mark of five or above, over ten, by using the weighted average, the final
mark will be 4.5 if a least a grade of 4 over ten is not obtained in each of
the two parts of the final exam In both opportunities, a final grade of five
over ten is required to pass the subject. 
The final grade is calculated by
considering all assessable activities and applying the weights indicated above. 
Matricula de Honor
(MH). An extra exam will be carried out in case of
the number of student students, eligible for Matrícula de Honor, is greater
than the number of allowed MHs. Students assessed in the second opportunity
could also be eligible for Matrícula de Honor if the maximum allowed number of
MHs has not been fully covered in the first opportunity.

Part-time students and those exempted from
attending classes. It is necessary for students to inform
the teacher at the beginning of the course.
 "NORMA QUE REGULA Ou RÉXIME DE DEDICACIÓN AO ESTUDO DÚAS ESTUDANTES DE GRAO NA UDC (Arts. 2.3; 3.b; 4.3 e 7.5) (04/05/2017) poderá realizar a proba mixta, sempre e cando os profesores sexan debidamente informados ao principio do curso. Sen menoscabo do anterior, os profesores poderán encargarlle a este alumnado diferentes traballos/problemas ó longo do curso para ser expostos en horario de titorias.




Sources of information
Basic Dahm, Donald J. (2012). Interpreting diffuse reflectance and transmitance : a theoretical introduction to diffuse reflectance and transmission in absorption spectroscopy of scattering materials. Chichester : NIR Publicaions
Ellis, Andrew M. (2005). Electronic and photoelectron spectroscopy fundamentals and case studies.. Cambridge University Press
P. R. Griffiths (2007). Fourier transform infrared spectrometry. John Wiley & Sons
G. Socrates (2005). Infrared and raman characteristic group frequencies tables and charts.. John Wiley & Sons
Smith, Ewen (2019). Modern Raman spectroscopy : a practical approach. Hoboken, NJ
Schlücker, Sebastian (2011). Surface enhanced Raman spectroscopy : analytical, biophysical and life science applications. Weinheim : Wiley-VCH

Estas son posibles fontes de información que poderes atopar no catálogo da biblioteca da UDC. Poderán suxerirse na plataforma de teleformación MOODLE,outras que ó longo do curso se consideren interesantes.

Complementary


Recommendations
Subjects that it is recommended to have taken before
Techniques of Characterisation of Nanomaterials 1/610G04025
Synthesis and Preparation of Nanomaterials/610G04020
Instrumental Analysis/610G04014
Fundamentals of Quantum Theory/610G04015
Spectroscopy/610G04017
Crystallography and Symmetry/610G04006

Subjects that are recommended to be taken simultaneously

Subjects that continue the syllabus
Nanotechnology in Pharmacy/610G04043
Nanotechnology in Food Industry/610G04044
Nanotechnology in Civil Engineering/610G04045
Nanotechnology in Medicine/610G04037
Nanotechnology in Environmental Science/610G04038
Nanofabrication/610G04040

Other comments


(*)The teaching guide is the document in which the URV publishes the information about all its courses. It is a public document and cannot be modified. Only in exceptional cases can it be revised by the competent agent or duly revised so that it is in line with current legislation.